Caffeine-loaded Fe3O4 nanoparticles: A new magnetically recoverable organocatalyst for Knoevenagel condensation reaction

Document Type: Original Research Paper

Author

Associate prof. of organic chemistry, Islamic Azad University of Mahshahr, Mahshahr, Iran

10.22034/jna.2018.576272.1110

Abstract

Caffeine loaded magnetic nanoparticle was successfully synthesized and were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis (EDX), thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and vibrating sample magnetometry (VSM). The resulting nanocomposite is shown to be an efficient catalyst in Knoevenagel condensations of various aldehydes under ultrasound irradiation.
Caffeine loaded magnetic nanoparticle was successfully synthesized and were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis (EDX), thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and vibrating sample magnetometry (VSM). The resulting nanocomposite is shown to be an efficient catalyst in Knoevenagel condensations of various aldehydes under ultrasound irradiation.
Caffeine loaded magnetic nanoparticle was successfully synthesized and were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis (EDX), thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and vibrating sample magnetometry (VSM). The resulting nanocomposite is shown to be an efficient catalyst in Knoevenagel condensations of various aldehydes under ultrasound irradiation.

Keywords